HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 2-Chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264344 | — |
| Edukt | N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline | HCID 20264352 | — |
| Edukt | Sodium Hypochlorite | HCID 23665760 | — |
| Produkt | 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide | HCID 53750274 | — |
Reaktionsschritte
Following the procedure of Example 4, N-methylcarbonyl 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline is converted, by reaction with HCl, to 2-chloro-3-(2,4-dichlorophenoxy)-6-nitroaniline, which is then reacted with potassium hydroxide and sodium hypochlorite, again following Example 4 procedures, to yield the final product, 4-chloro-5-(2,4-dichlorophenoxy)benzo-2,1,3-oxadiazole N-oxide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04544400 |
| Quelldatensatz | uspto-grants-1985_10 |
| ORD ID | ord-04bce43b8f9d420aa740cc9c2e7931dd |
| Quellennotiz | uspto-grants-1985_10 |