Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Edukt | Monomethyl azelate | HCID 75009 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | Methyl 9-chloro-9-oxononanoate | HCID 544297 | — |
Reaktionsschritte
In a separate process, 23.9 g of azelaic monomethylester was dissolved in 30 ml chloroform. Oxalylchloride (15 ml) was added, all at once, and the mixture refluxed 2 hours at 50° C. The mixture was cooled; excess solvent and oxalylchloride were evaporated. After distillation, 25.8 g of CH3OCO(CH2)7COCl was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US04544668 |
|---|
| Quelldatensatz | uspto-grants-1985_10 |
|---|
| ORD ID | ord-e70b7d36c96148e3b9e913f07b19395b |
|---|
| Quellennotiz | uspto-grants-1985_10 |
|---|
