Triphenylphosphine → (Ethoxymethyl)(triphenyl)phosphanium chloride

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

A solution of 99.66 g of triphenylphosphine and 37.82 g of chloromethyl ethyl ether in 240 ml of dry benzene was stirred and refluxed (84° C.) for 6 hours. The mixture then was chilled and filtered to give 7, as a white solid, mp 205°-206° C.

Herkunft & Nachweise