HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
[6-(Hydroxymethyl)pyridin-3-yl]methanol → 5-(Hydroxymethyl)pyridine-2-carboxaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | [6-(Hydroxymethyl)pyridin-3-yl]methanol | HCID 820251 | — |
| Katalysator | HCID 178418406 | HCID 178418406 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 5-(Hydroxymethyl)pyridine-2-carboxaldehyde | HCID 13518562 | — |
Reaktionsschritte
2,5-Di(hydroxymethyl)pyridine (10 g.) in 300 ml. of hot chloroform is treated with 100 g of manganese dioxide. After 1/2 hour of stirring, the mixture is filtered and the filtrate is evaporated to dryness to give 2-formyl-5-hydroxymethylpyridine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04546106 |
| Quelldatensatz | uspto-grants-1985_10 |
| ORD ID | ord-bd310b86aab94d3a98f09655062f091e |
| Quellennotiz | uspto-grants-1985_10 |