HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thiophenol → N-benzyloxycarbonyl-glycine-phenythio ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thiophenol | HCID 7969 | — |
| Edukt | Benzyloxycarbonylglycine | HCID 14349 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | N-benzyloxycarbonyl-glycine-phenythio ester | HCID 22764889 | 62% |
Reaktionsschritte
Using thiophenol and Z-Gly.OH, Example 78 was repeated; except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl-glycine-phenythio ester (hereinafter represented by ##STR12## in a yield of 62%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04173563 |
| Quelldatensatz | uspto-grants-1979_11 |
| ORD ID | ord-01bd8ea14e7b4957854705e522f04f34 |
| Quellennotiz | uspto-grants-1979_11 |