HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyl-(2-piperidin-2-yl-ethyl)-amine → 5,10-Dihydro-5-[[2-[2-(dimethylamino)ethyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyl-(2-piperidin-2-yl-ethyl)-amine | HCID 296295 | — |
| Edukt | 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 10085419 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 5,10-Dihydro-5-[[2-[2-(dimethylamino)ethyl]-1-piperidinyl]-acetyl]-11H-dibenzo[b,e][1,4]diazepin-11-one | HCID 13578559 | — |
Reaktionsschritte
The title compound is prepared analogously to Example 2 from 5-(chloroacetyl)-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-one and 2-[2-(dimethylamino)ethyl]piperidine to give colorless crystals, mp. 155°-157° C. (acetonitrile).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04550107 |
| Quelldatensatz | uspto-grants-1985_10 |
| ORD ID | ord-60e390bd0a8b45b6a7d430164a616997 |
| Quellennotiz | uspto-grants-1985_10 |