Acetic Anhydride → N-[2-[[2,6-bis(1-Methylethyl)phenyl]amino]-2-oxoethyl]-N-(diphenylmethyl)-2,2,3,3,4,4,4-heptafluorobutanamide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Acetic Anhydride	HCID 7918	—
Edukt	Heptafluorobutyric anhydride	HCID 67643	—
Edukt	N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide	HCID 1645639	—
Edukt	N-[2,6-bis(1-Methylethyl)phenyl]-2-[(1,1-dimethyl-2-phenylethyl)amino]acetamide	HCID 19874910	—
Produkt	N-[2-[[2,6-bis(1-Methylethyl)phenyl]amino]-2-oxoethyl]-N-(diphenylmethyl)-2,2,3,3,4,4,4-heptafluorobutanamide	HCID 19874870	—

Reaktionsschritte

When in the procedure of Example 79 an appropriate amount of the product of Example 4 was substituted for the product of Example 5 and an appropriate amount of heptafluorobutyric anhydride was substituted for acetic anhydride and the general procedure of Example 79 was followed the title compound was obtained. Total yield, 1.33 g (59%).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US05153226
Quelldatensatz	uspto-grants-1992_10
ORD ID	ord-dc87ba1364ec41c1901f800b265ed00b
Quellennotiz	uspto-grants-1992_10