2,5-Dimethoxybenzoyl chloride → N-[2-[(2,6-Diethylphenyl)amino]-2-oxoethyl]-N-(diphenylmethyl)benzamide

HRID 465662

Reaktionsgleichung

Reaktionsgleichung von HRID 465662
[CH3:1][CH:2]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10](C)[CH3:11])[C:5]=1[NH:13][C:14](=[O:30])[CH2:15][NH:16][CH:17]([C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)C.CO[C:33]1[CH:41]=[CH:40][C:39](OC)=[CH:38][C:34]=1[C:35](Cl)=[O:36].COC1C=CC=CC=1C(Cl)=O>>[CH2:10]([C:6]1[CH:7]=[CH:8][CH:9]=[C:4]([CH2:2][CH3:1])[C:5]=1[NH:13][C:14](=[O:30])[CH2:15][N:16]([CH:17]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:24]1[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=1)[C:35](=[O:36])[C:34]1[CH:33]=[CH:41][CH:40]=[CH:39][CH:38]=1)[CH3:11]

Komponenten

4

Edukt 3

HCID 873642,5-Dimethoxybenzoyl chlorideHCID 889692-Methoxybenzoyl chlorideHCID 1645639N-[2,6-bis(1-Methylethyl)phenyl]-2-[(diphenylmethyl)amino]acetamide

Produkt 1

HCID 19874973N-[2-[(2,6-Diethylphenyl)amino]-2-oxoethyl]-N-(diphenylmethyl)benzamide

Versuchsvorschrift

When in the procedure of Example 94 an appropriate amount of the product of Example 75 was substituted for the product of Example 4 and an appropriate amount of 2,5-dimethoxybenzoyl chloride was substituted for 2-methoxybenzoyl chloride and the general procedure of Example 94 was followed the title compound was obtained. Total yield, 0.35 g (51%).

Quellen und Nachweise

ORD-Eintrag
ord-e1d2905f9dd141739d0344d26637e187
Quelldatensatz
uspto-grants-1992_10
Patentnummer
US05153226

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