HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4,5-Trimethoxybenzaldehyde → N,N-Dimethyl-N'-[(3,4,5-trimethoxyphenyl)methylene]-1,3-propanediamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4,5-Trimethoxybenzaldehyde | HCID 6858 | — |
| Edukt | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | N,N-Dimethyl-N'-[(3,4,5-trimethoxyphenyl)methylene]-1,3-propanediamine | HCID 20386241 | 94% |
Reaktionsschritte
Interaction of 21 g of 3,4,5-trimethoxybenzaldehyde with 11 g of 3-dimethylaminopropylamine in 80 ml. of benzene following the procedure described in Example 1 yields 28.2 g of product as an oil, boiling point 162°-167° C. at 0.4-0.5 mm. of Hg.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04174317 |
| Quelldatensatz | uspto-grants-1979_11 |
| ORD ID | ord-4b3cc334fad24d0e82410294c773b13e |
| Quellennotiz | uspto-grants-1979_11 |