HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Octene → Gamma-Decalactone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Octene | HCID 8125 | — |
| Edukt | Potassium Acetate | HCID 517044 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | Gamma-Decalactone | HCID 12813 | 48% |
Reaktionsschritte
Octene-1 in an amount of 2.2 g. and 23.6 g. of ceric ammonium nitrate, Ce(NH4)2 (NO3)6, were refluxed under nitrogen in 200 ml. glacial acetic acid containing 60 g. potassium acetate for less than 0.5 hour, there being obtained a 48% yield of gamma-n-hexyl-butyrolactone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04175089 |
| Quelldatensatz | uspto-grants-1979_11 |
| ORD ID | ord-2c03d4a37bfe48c9975a949c07039ab8 |
| Quellennotiz | uspto-grants-1979_11 |