Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | 4-Bromophenol | HCID 7808 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | (Chloromethyl)cyclopropane | HCID 80013 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 1-Bromo-4-(cyclopropylmethoxy)benzene | HCID 15625752 | — |
Reaktionsschritte
5.0 g (28.9 mmol) 4-bromophenol, 3.93 g (43.4 mmol) (chloromethyl)cyclopropane and 7.99 g (57.8 mmol) K2CO3 are added to 10 mL DMF and stirred at 80° C. over night. Afterwards the reaction mixture is diluted with water and extracted with DCM. The organic layer is dried with MgSO4, filtered and the solvent is removed in vacuo.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08623860B2 |
|---|
| Quelldatensatz | uspto-grants-2014_01 |
|---|
| ORD ID | ord-e2a0d5eb27f54a2c8c9fae9d97057072 |
|---|
| Quellennotiz | uspto-grants-2014_01 |
|---|
