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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 46753Erstellt: 23. Oktober 2026

Benzaldehyde → Cyano(phenyl)methyl 2-methylpropanoate

https://huagongshe.com/de/reaction/46753

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzaldehydeHCID 240—
EduktIsobutyric anhydrideHCID 7346—
EduktSodium CyanideHCID 8929—
LösungsmittelWaterHCID 962—
ProduktCyano(phenyl)methyl 2-methylpropanoateHCID 13536647—

Reaktionsbedingungen

Temperatur25 °C

Reaktionsschritte

A 100-ml round-bottomed flask equipped with a magnetic stirrer was charged with isobutyric anhydride (10 mmol), benzaldehyde (10 mmol), a mixture of alkanes (25 ml) having a boiling range of from 62° C. to 82° C., sodium cyanide (12 mmol) and water (3 ml). The mixture formed was stirred at a temperature of 25° C. The table presents the yields of the title ester after the reaction times indicated (Embodiment IV).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04175094
Quelldatensatzuspto-grants-1979_11
ORD IDord-b8b0d7af08bb45c5b88e08b5a8efd0a7
Quellennotizuspto-grants-1979_11