HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylformamide → (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | Dimethylacetamide | HCID 31374 | — |
| Edukt | 1-Fluoro-5-methyl-2,4-dinitrobenzene | HCID 520705 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine | HCID 15022335 | 63% |
Reaktionsbedingungen
| Temperatur | 100 °C |
|---|
Reaktionsschritte
A mixture of 1-fluoro-5-methyl-2,4-dinitro-benzene (10 g, 50 mmol), DMA (12 g, 100 mmol) and DMF (50 nit) was heated at 100° C. for 4 h. The solution was cooled and poured into water. The precipitated red solid was collected, washed with water, and dried to give (E)-2-(5-fluoro-2,4-dinitrophenyl)-N,N-dimethylethenamine (8.0 g, 63%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08623905B2 |
| Quelldatensatz | uspto-grants-2014_01 |
| ORD ID | ord-b8df435da39b42fd8e4410c5ca578235 |
| Quellennotiz | uspto-grants-2014_01 |