HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Bromide → 1-benzyl-1H-indol-6-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Bromide | HCID 7498 | — |
| Edukt | 6-Nitro-1H-indole | HCID 78502 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 1-benzyl-1H-indol-6-amine | HCID 22019562 | — |
Reaktionsschritte
1-Benzyl-1H-indol-6-ylamine (B-2) was synthesized following the general scheme above starting from 6-nitroindole and benzyl bromide. Overall yield (˜40%). HPLC ret. time 2.19 min, 10-99% CH3CN, 5 min run; ESI-MS 223.3 m/z (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08629162B2 |
| Quelldatensatz | uspto-grants-2014_01 |
| ORD ID | ord-3387cbe5db1a4a9c9152916ea4cf6982 |
| Quellennotiz | uspto-grants-2014_01 |