Dimethylformamide → N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine

HRID 47062

Reaktionsgleichung

[CH3:1][C:2]1[C:7]([C:8]#[N:9])=[CH:6][CH:5]=[CH:4][N:3]=1.[CH3:10][N:11]([CH:13]=O)[CH3:12]>>[CH3:10][N:11]([CH3:13])[CH:12]=[CH:1][C:2]1[C:7]([C:8]#[N:9])=[CH:6][CH:5]=[CH:4][N:3]=1

Komponenten

Edukt 2

HCID 6228Dimethylformamide

HCID 47383082-Methylpyridine-3-carbonitrile

Produkt 1

HCID 54435625N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine

Versuchsvorschrift

N,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared using the procedure of 4 A from 2-methyl-3-cyanopyridine (9.0 g, 0.076 m), DMF acetal (11.0 g, 0.092 m) and DMF (50 mL) yielding N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine b.p.=133°-135° (0.3 mm), m.p.=49°-50° after sublimation at 50° (0.3 mm).

Aufarbeitung

customN,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared

Quellen und Nachweise

ORD-Eintrag: ord-4a2635ef6c464657ae9922b89defc428
Quelldatensatz: uspto-grants-1979_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04176183

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