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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 47084Erstellt: 23. Oktober 2026

Phenol → Phenyl 4-chloro-3-nitrobenzenesulfonate

https://huagongshe.com/de/reaction/47084

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPhenolHCID 996—
EduktBenzenesulfonyl chloride, 4-chloro-3-nitro-HCID 7323—
Edukt2-Amino-4-phenoxysulfonyl-butyranilideHCID 20385152—
ProduktPhenyl 4-chloro-3-nitrobenzenesulfonateHCID 266121—

Reaktionsschritte

Thus, for example, 2-amino-4-phenoxysulfonyl-butyranilide can be obtained by reacting 3-nitro-4-chloro-benzene-sulfonic acid-chloride with phenol to yield 2-nitro-4-phenoxysulfonylchloro-benzene, reacting this product with ammonia to give 2-nitro-4-phenoxy-sulfonyl-aniline, acylating this compound with butyryl-chloride to form 2-nitro-4-phenoxysulfonyl-butyranilide, and by subsequently hydrogenating said product catalytically.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04176192
Quelldatensatzuspto-grants-1979_11
ORD IDord-42b221de0f3d4aa6a91e834c6f98940c
Quellennotizuspto-grants-1979_11