2-Methoxy-4-(methylthio)benzoyl chloride → 4,4-Dimethyl-7-(2-methoxy-4-methylmercapto-benzoylamino)-8-nitro-2H,4H-isoquinoline-1,3-dione

HRID 47106Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 47106
[CH3:1][C:2]1([CH3:18])[C:11]2[C:6](=[C:7]([N+:13]([O-:15])=[O:14])[C:8]([NH2:12])=[CH:9][CH:10]=2)[C:5](=[O:16])[NH:4][C:3]1=[O:17].[CH3:19][O:20][C:21]1[CH:29]=[C:28]([S:30][CH3:31])[CH:27]=[CH:26][C:22]=1[C:23](Cl)=[O:24]>>[CH3:1][C:2]1([CH3:18])[C:11]2[C:6](=[C:7]([N+:13]([O-:15])=[O:14])[C:8]([NH:12][C:23](=[O:24])[C:22]3[CH:26]=[CH:27][C:28]([S:30][CH3:31])=[CH:29][C:21]=3[O:20][CH3:19])=[CH:9][CH:10]=2)[C:5](=[O:16])[NH:4][C:3]1=[O:17]

Komponenten

3

Edukt 2

HCID 27595912-Methoxy-4-(methylthio)benzoyl chlorideHCID 111184431,3(2H,4H)-Isoquinolinedione, 7-amino-4,4-dimethyl-8-nitro-

Produkt 1

HCID 538613404,4-Dimethyl-7-(2-methoxy-4-methylmercapto-benzoylamino)-8-nitro-2H,4H-isoquinoline-1,3-dione

Versuchsvorschrift

Prepared analogous to Example 2a from 5 gm of 4,4-dimethyl-7-amino-8-nitro-2H,4H-isoquinoline-1,3-dione and 2-methoxy-4-methylmercapto-benzoyl chloride.

Quellen und Nachweise

ORD-Eintrag
ord-6bd245d460a4453d97956dfb904b5bdb
Quelldatensatz
uspto-grants-1979_11
Patentnummer
US04176184

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