HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,9-Nonanediol → 2-(9-Hydroxynonyloxy)-6-nitrobenzonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,9-Nonanediol | HCID 19835 | — |
| Edukt | 1,1,3,3-Tetramethylguanidine | HCID 66460 | — |
| Edukt | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Edukt | Dinitrobenzonitrile | HCID 520718 | — |
| Produkt | 2-(9-Hydroxynonyloxy)-6-nitrobenzonitrile | HCID 66745844 | 30,7% |
Reaktionsschritte
Prepared as in Example 274c (except DBU was replaced with 1,1,3,3-tetramethylguanidine) from 1,9-nonanediol and 2,6-dinitrobenzonitrile in 30.7% yield. MS 307 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08633186B2 |
| Quelldatensatz | uspto-grants-2014_01 |
| ORD ID | ord-076f53052f25463eb13a0e32111033ae |
| Quellennotiz | uspto-grants-2014_01 |