HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Isobutyl Methacrylate → 2-Methylundecane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Isobutyl Methacrylate | HCID 7352 | — |
| Edukt | Lauryl Methacrylate | HCID 8906 | — |
| Produkt | 2-Methylundecane | HCID 23459 | — |
Reaktionsschritte
24 g of helio fast blue HG (C.I. no. 74160), 6 g of a copolymer formed from 75% of lauryl methacrylate and 25% of isobutyl methacrylate with a molecular weight of 150 000, and 210 g of isododecane are mixed for 10 hours using a bead vibrating mill. 100 g of the dispersion obtained are diluted with 100 g of isododecane and reacted with vigorous stirring over a period of 30 minutes at 25° C. with a mixture of 4.5 g of isobutyl cyanoacrylate and 1.5 g of allyl cyanoacrylate. The dispersion was stirred for a further 2 hours at 25° C., then centrifuged and the isolated solid matter was washed with isododecane, centrifuged again and dried. 30 g of coated blue pigment are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04885191 |
| Quelldatensatz | uspto-grants-1989_12 |
| ORD ID | ord-3271b50f447942e882da04bdbcbed58e |
| Quellennotiz | uspto-grants-1989_12 |