HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Hydroxide → HCID 19836535, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | p-Toluenesulfonic acid 1-methylheptyl ester | HCID 3912199 | — |
| Edukt | 3'-Bromo-4'-hydroxy-4-acetylbiphenyl | HCID 14474361 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 19836535 | HCID 19836535 | — |
Reaktionsschritte
The above 3'-bromo-4'-hydroxy-4-acetylbiphenyl (200 g) was treated with 1.2 times equivalents of R 1-methylheptyl p-toluenesulfonate and potassium hydroxide in 97% ethanol (1 l) for 6 hours under reflux. The reaction mixture was worked up in a usual way to obtain crude oily 3'-bromo-4'-(1-methylheptyloxy)-4-acetylbiphenyl (163 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04886622 |
| Quelldatensatz | uspto-grants-1989_12 |
| ORD ID | ord-a1bd88eaf8ec4544ad9ec66057274992 |
| Quellennotiz | uspto-grants-1989_12 |