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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 476825Erstellt: 25. Oktober 2026

Potassium Hydroxide → HCID 19836535, Verbindung

https://huagongshe.com/reaction/476825

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPotassium HydroxideHCID 14797—
Eduktp-Toluenesulfonic acid 1-methylheptyl esterHCID 3912199—
Edukt3'-Bromo-4'-hydroxy-4-acetylbiphenylHCID 14474361—
LösungsmittelEthanolHCID 702—
ProduktHCID 19836535HCID 19836535—

Reaktionsschritte

The above 3'-bromo-4'-hydroxy-4-acetylbiphenyl (200 g) was treated with 1.2 times equivalents of R 1-methylheptyl p-toluenesulfonate and potassium hydroxide in 97% ethanol (1 l) for 6 hours under reflux. The reaction mixture was worked up in a usual way to obtain crude oily 3'-bromo-4'-(1-methylheptyloxy)-4-acetylbiphenyl (163 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04886622
Quelldatensatzuspto-grants-1989_12
ORD IDord-a1bd88eaf8ec4544ad9ec66057274992
Quellennotizuspto-grants-1989_12