Benzylamine → Benzeneacetamide, 4-hydroxy-N-(phenylmethyl)-

HRID 476853Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 476853
CO[C:3](=[O:12])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([OH:11])=[CH:7][CH:6]=1.[CH2:13]([NH2:20])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[CH2:13]([NH:20][C:3](=[O:12])[CH2:4][C:5]1[CH:6]=[CH:7][C:8]([OH:11])=[CH:9][CH:10]=1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Komponenten

3

Edukt 2

HCID 7504BenzylamineHCID 518900Benzeneacetic acid, 4-hydroxy-, methyl ester

Produkt 1

HCID 8376026Benzeneacetamide, 4-hydroxy-N-(phenylmethyl)-

Versuchsvorschrift

A mixture of 80 g of 4-hydroxyphenylacetic acid methyl ester and 51.6 g of benzylamine is brought to 180° C. for 8 hours. The mixture is allowed to return to room temperature and the crystals are filtered off and washed with ethanol and then ethyl ether.

Aufarbeitung

  1. customto return to room temperature
  2. filtrationthe crystals are filtered off
  3. washwashed with ethanol

Quellen und Nachweise

ORD-Eintrag
ord-467e9f33b6914da9b3e0388437aff99c
Quelldatensatz
uspto-grants-1989_12
Patentnummer
US04886799

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