2-Nitrophenol → HCID 15017530, Verbindung

HRID 477268

Reaktionsgleichung

Reaktionsgleichung von HRID 477268
[Cl:1][C:2]1[C:3](F)=[N:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1.[N+:13]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[OH:22])([O-:15])=[O:14]>>[Cl:1][C:2]1[C:3]([O:22][C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=2[N+:13]([O-:15])=[O:14])=[N:4][CH:5]=[C:6]([C:8]([F:11])([F:10])[F:9])[CH:7]=1

Komponenten

3

Edukt 2

HCID 69472-NitrophenolHCID 12680753-Chloro-2-fluoro-5-(trifluoromethyl)pyridine

Produkt 1

HCID 15017530HCID 15017530, VerbindungAusbeute 63 %

Versuchsvorschrift

This material was prepared in 63% yield from 3-chloro-2-fluoro-5-trifluoromethylpyridine and 2-nitrophenol following the general procedure outlined in Example 104. The product was isolated as an amber oil which was characterized by IR and 1H NMR spectroscopy.

Aufarbeitung

  1. customThe product was isolated as an amber oil which

Quellen und Nachweise

ORD-Eintrag
ord-ee74605885a04bcebaa429762abca957
Quelldatensatz
uspto-grants-1989_12
Patentnummer
US04886883

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