Allyl isocyanate → alpha-Allylcarbamoyl-beta-cyclopropyl-beta-oxopropionitrile

Beteiligte Stoffe

Reaktionsschritte

When β-cyclopropyl-β-oxopropionitrile (2,.00 g, 18.3 mmoles) [prepared in Example 1, Step A]was reacted with allylisocyanate (1.60 g, 19.2 mmoles) according to the general procedure of Example 1, Sep B, the title compound (2.8 g) was obtained as a white solid after recrystallization from 30% aqueous ethanol, m.p. 72°-73.5° C.

Herkunft & Nachweise