2-Chloropyrimidine → HCID 19872288, Verbindung
Reaktionsgleichung
[CH2:1]([S:8][C:9]1[N:13]=[C:12]([S:14][CH3:15])[NH:11][N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[C:17]1[N:22]=[CH:21][CH:20]=[CH:19][N:18]=1>>[CH2:1]([S:8][C:9]1[N:13]=[C:12]([S:14][CH3:15])[N:11]([C:17]2[N:22]=[CH:21][CH:20]=[CH:19][N:18]=2)[N:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Komponenten
3
Versuchsvorschrift
The product of stage (a) (50 g) was treated with 2-chloropyrimidine (24.4 g) in a method analogous to that of Example F, to give, after chromatographic separation of two products, 23.6 g of the desired product.
Aufarbeitung
- customto give
- customafter chromatographic separation of two products, 23.6 g of the desired product
Quellen und Nachweise
- ORD-Eintrag
- ord-46190c8f1da14c1a8cb9abdc2e881651
- Quelldatensatz
- uspto-grants-1989_12
- Patentnummer
- US04889553
Notizen zur Reaktion
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