HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Hydroxide → Potassium cinnamate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | Cinnamyl Alcohol | HCID 5315892 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | Potassium cinnamate | HCID 44135689 | — |
Reaktionsschritte
50 g (0,36 mol) of cinnamic alcohol are dissolved in 180 ml of dry toluene. 20 g (0,36 mol) of KOH are added to the solution, and the resulting mixture is kept under stirring for one hour at room temperature. During this phase, potassium cinnamate is obtained. Then, a solution prepared starting from 18 g (0,10 mol) of 2,4,6-trichloro-s-triazine in 150 ml of toluene is added, allowing to react at room temperature for further 90 hours under stirring.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06645396B2 |
| Quelldatensatz | uspto-grants-2003_11 |
| ORD ID | ord-4f889249f22e44c297275e8a0c6e5abd |
| Quellennotiz | uspto-grants-2003_11 |