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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 47944Erstellt: 25. Oktober 2026

1-Methylimidazole → HCID 178448538, Verbindung

https://huagongshe.com/reaction/47944

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-MethylimidazoleHCID 1390—
EduktButyl ChlorideHCID 8005—
ProduktHCID 178448538HCID 17844853898,3%

Reaktionsbedingungen

Temperatur60 °C

Reaktionsschritte

251.4 g of 1-chlorobutane (2.7 mol) are loaded into a 1 l glass reactor. The mixture is heated to 60° C., and then 148.6 g of 1-methylimidazole (1.8 mol) are poured in dropwise, with stirring. The mixture is left to react for 24 h at 80° C. The reaction mixture is evaporated under vacuum. 309 g of 1-butyl-3-methylimidazolium chloride are obtained in the form of a yellowish solid (yield=98%). The product is used as it is without further purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06700007B2
Quelldatensatzuspto-grants-2004_03
ORD IDord-68bc9c3131dd4c65bf273fb78a69005b
Quellennotizuspto-grants-2004_03