HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 47944Erstellt: 25. Oktober 2026
1-Methylimidazole → HCID 178448538, Verbindung
https://huagongshe.com/reaction/47944
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 1-Methylimidazole | HCID 1390 | — |
| Edukt | Butyl Chloride | HCID 8005 | — |
| Produkt | HCID 178448538 | HCID 178448538 | 98,3% |
Reaktionsschritte
251.4 g of 1-chlorobutane (2.7 mol) are loaded into a 1 l glass reactor. The mixture is heated to 60° C., and then 148.6 g of 1-methylimidazole (1.8 mol) are poured in dropwise, with stirring. The mixture is left to react for 24 h at 80° C. The reaction mixture is evaporated under vacuum. 309 g of 1-butyl-3-methylimidazolium chloride are obtained in the form of a yellowish solid (yield=98%). The product is used as it is without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06700007B2 |
|---|
| Quelldatensatz | uspto-grants-2004_03 |
|---|
| ORD ID | ord-68bc9c3131dd4c65bf273fb78a69005b |
|---|
| Quellennotiz | uspto-grants-2004_03 |
|---|