HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 480409Erstellt: 23. Oktober 2026
Methyl iodide → 2-Amino-4-(3,5-diacetylphenyl)amino-1,6-dimethylpyrimidinium iodide
https://huagongshe.com/de/reaction/480409
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | Cni H1194 | HCID 133109 | — |
| Lösungsmittel | Acetonitrile tetrahydrofuran | HCID 22177404 | — |
| Produkt | 2-Amino-4-(3,5-diacetylphenyl)amino-1,6-dimethylpyrimidinium iodide | HCID 9845352 | — |
Reaktionsschritte
Compound No. 2, FIG. 1A: A suspension of Compound No. 11 (2-amino-4-(3,5-diacetylphenyl)amino-6-methylpyrimidine) (0.284 g), was suspended in 1:1 acetonitrile-tetrahydrofuran was treated with methyl iodide (2 mL) and heated at 40-45° C. under a reflux condenser for 18 hr. Cooling and filtration gave 0.35 g of 2-amino-4-(3,5-diacetylphenyl)amino-1,6-dimethylpyrimidinium iodide, mp 292° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US06649797B2 |
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| Quelldatensatz | uspto-grants-2003_11 |
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| ORD ID | ord-c592da5037114eec80d273c9922a3f21 |
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| Quellennotiz | uspto-grants-2003_11 |
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