HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Naphthylamine → 2-[N-(naphth-2-yl)amino]butanoic Acid Ethyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Naphthylamine | HCID 7057 | — |
| Edukt | Butanoic acid, 2-bromo-, ethyl ester | HCID 79039 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 2-[N-(naphth-2-yl)amino]butanoic Acid Ethyl Ester | HCID 10131322 | — |
Reaktionsschritte
Following General Procedure AJ above and using 2-aminonaphthalene (Aldrich) and ethyl 2-bromobutyrate (Aldrich), the title compound was prepared as a solid, m.p. 81-83° C. The reaction was monitored by silica gel tlc (Rf=0.5 in CHCl3). Purification was by chromatography (silica gel using chloroform as the eluant).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06653303B1 |
| Quelldatensatz | uspto-grants-2003_11 |
| ORD ID | ord-2aca0f4386354c6ea8c2ece27253a938 |
| Quellennotiz | uspto-grants-2003_11 |