HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Uridine → 5'-O-(4-Methylbenzoyl)uridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Uridine | HCID 6029 | — |
| Edukt | 4-Methylbenzoyl Chloride | HCID 13405 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | 5'-O-(4-Methylbenzoyl)uridine | HCID 11588577 | — |
Reaktionsschritte
4-Methylbenzoyl chloride (10 mmol) is added to a solution of uridine (10 mmol) in 20 mL of pyridine. After no further progress occurs as observed by TLC, the volatile components are evaporated in vacuo. The residue is purified using flash chromatography to give the product as a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06702705B1 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-5fea9a53770246ee989f9ac9adc592d9 |
| Quellennotiz | uspto-grants-2004_03 |