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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 482970Erstellt: 26. Oktober 2026

Thiamine Hydrochloride → thiazolium, 3-((4-amino-2-methyl-5-pyrimidinyl)methyl)-5-(2-hydroxyethyl)-4-methyl-, salt with 1,2,3,4-tetrahydro-2-methyl-1,4-dioxo-2-naphthalenesulfonic acid (1:1), mono(1,2,3,4-tetrahydro-2-methyl-1,4-dioxo-2-naphthalenesulfonate) (salt)

https://huagongshe.com/reaction/482970

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktThiamine HydrochlorideHCID 6202—
EduktMenadione Sodium BisulfiteHCID 23665888—
LösungsmittelWaterHCID 962—
Produktthiazolium, 3-((4-amino-2-methyl-5-pyrimidinyl)methyl)-5-(2-hydroxyethyl)-4-methyl-, salt with 1,2,3,4-tetrahydro-2-methyl-1,4-dioxo-2-naphthalenesulfonic acid (1:1), mono(1,2,3,4-tetrahydro-2-methyl-1,4-dioxo-2-naphthalenesulfonate) (salt)HCID 121232542—

Reaktionsschritte

25 g of thiamine hydrochloride (vitamin B1) was dissolved in 50 g of water; to said solution of 25 g of powdery sodium menadione bisulfite was added within about half an hour. After half an hour of agitation, the reaction mass became opalescent and the adduct began to precipitate. After an hour, the precipitate was filtered, washed and dried. 25 g of a white product having the following analysis was obtained.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04577019
Quelldatensatzuspto-grants-1986_03
ORD IDord-a76a9e7bad3d40479e682b9c4056a987
Quellennotizuspto-grants-1986_03