Thionyl Chloride → 2-(Octyloxy)benzoyl chloride

Reaktionsgleichung

[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12](O)=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:21])=O>>[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][CH:16]=[CH:15][C:11]=1[C:12]([Cl:21])=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Komponenten

Edukt 2

HCID 24386Thionyl Chloride

HCID 200827752-(Octyloxy)benzoic acid

Produkt 1

HCID 203111572-(Octyloxy)benzoyl chloride

Versuchsvorschrift

First, octyloxybenzoic acid was heated in thionyl chloride under reflux until complete dissolution. Excess thionyl chloride was removed by vacuum distillation. Thus there was obtained octyloxybenzoic acid chloride.

Aufarbeitung

temperatureunder reflux until complete dissolution
customExcess thionyl chloride was removed by vacuum distillation

Quellen und Nachweise

ORD-Eintrag: ord-65b436956dee4667b9a4e64adcfcd867
Quelldatensatz: uspto-grants-1993_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05225105

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