Perfluoropropionyl fluoride → 1,1,1,3,3,4,4,4-Octafluoro-2-(trifluoromethyl)-2-butanol

HRID 483915

Reaktionsgleichung

[F-:1].[K+].[F:3][C:4]([F:12])([C:8]([F:11])([F:10])[F:9])[C:5](F)=[O:6]>C(#N)C>[F:1][C:4]([F:12])([F:3])[C:5]([C:8]([F:11])([F:10])[F:9])([OH:6])[C:4]([F:12])([F:3])[C:8]([F:11])([F:10])[F:9]

Komponenten

Reaktionsbedingungen

Temperatur: -196 °C

Versuchsvorschrift

By operating as in the above examples, 0.26 g of KF (4.5 mmol) was charged to the reactor, and then 4.0 ml of anhydrous acetonitrile was injected through the pierceable cap; the whole was then cooled down to -196° C. with the residual air being evacuated; then, 2.0 mmol of pentafluoropropionyl fluoride

Aufarbeitung

additionwas charged to the reactor
custombeing evacuated

Quellen und Nachweise

ORD-Eintrag: ord-26b6efaca80344a497d3f837a6d8c214
Quelldatensatz: uspto-grants-1993_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05227539

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