Thionyl Chloride → HCID 53411290, Verbindung

HRID 483941Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 483941
[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7](O)=[O:8].S(Cl)([Cl:15])=O>C1C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7]([Cl:15])=[O:8]

Komponenten

4

Edukt 2

HCID 24386Thionyl ChlorideHCID 746313-(3-Chlorophenyl)prop-2-enoic acid

Produkt 1

HCID 53411290HCID 53411290, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 241BenzeneLösungsmittel

Versuchsvorschrift

100 ml of benzene was added to 18.3 grams of m-chlorocinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 80° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.

Aufarbeitung

  1. customat ambient temperature
  2. customwas elevated to 80° C.
  3. distillationBenzene and thionyl chloride were distilled off
  4. customthe residue was dried thoroughly under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-05381250536a4912991c8429137f6a18
Quelldatensatz
uspto-grants-1993_07
Patentnummer
US05229002

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