HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → N-(2,3-Dihydro-1H-inden-2-yl)acetamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | 2-Aminoindane | HCID 76310 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | N-(2,3-Dihydro-1H-inden-2-yl)acetamide | HCID 12452137 | 71,1% |
Reaktionsschritte
2-aminoindan (6.0 g, 45 mmol) was dissolved in dry pyridine (7 ml), to which acetic anhydride (4.5 ml, 47.3 mmol) was added dropwise while cooling in ice water. After the reaction mixture was returned to room temperature and stirred for 20 minutes, water was added. The precipitate that deposited was filtered to obtain 2-acetamidoindan (5.6 g, 32 mmol).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06703421B1 |
| Quelldatensatz | uspto-grants-2004_03 |
| ORD ID | ord-98d057ea4c4f49e8bf8e66ae144e62ee |
| Quellennotiz | uspto-grants-2004_03 |