2,6-Dimethyl-4-nitroaniline → 2-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

HRID 484787

Reaktionsgleichung

Reaktionsgleichung von HRID 484787
Cl[C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1.[CH3:7][C:8]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[C:11]([CH3:18])[C:9]=1[NH2:10]>>[CH3:7][C:8]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[C:11]([CH3:18])[C:9]=1[NH:10][C:2]1[CH2:6][CH2:5][CH2:4][N:3]=1

Komponenten

3

Edukt 2

HCID 281592,6-Dimethyl-4-nitroanilineHCID 135201412-Chloro-1-pyrroline

Produkt 1

HCID 202723942-[(2,6-Dimethyl-4-nitrophenyl)amino]-1-pyrroline

Versuchsvorschrift

A mixture of 2-chloro-1-pyrroline, prepared as in Example 1, and 19.9 g (0.12 mole) of the aniline product of Example 6 were heated at reflux overnight, according to the general method of Example 8. The title compound was isolated and used for subsequent reactions without further purification. Structure assignment was supported by nmr and infrared spectra.

Aufarbeitung

  1. temperaturewere heated
  2. temperatureat reflux overnight

Quellen und Nachweise

ORD-Eintrag
ord-b73808b27f264206b52ae5c5d7b1945f
Quelldatensatz
uspto-grants-1985_08
Patentnummer
US04533739

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