HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Iodide → N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Iodide | HCID 4875 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 12769237 | — |
| Edukt | N,N-diallyl alpha-bromopropionamide | HCID 13036601 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide | HCID 13503503 | — |
Reaktionsschritte
The reaction mixture was washed with water and dried and the solvent was distilled off to obtain 3.8 g. of N,N-diallyl α-bromopropionamide. The product was admixed with 3.5 g. of N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide, 2.2 g. of potassium carbonate, 1.8 g. of potassium iodide and 50 ml. of acetone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04536209 |
| Quelldatensatz | uspto-grants-1985_08 |
| ORD ID | ord-bf2d6795dd0b49899e460acfaecd3e6b |
| Quellennotiz | uspto-grants-1985_08 |