HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Toluenesulfonyl chloride → HCID 13957272, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Edukt | 1-Octanol, 8-chloro- | HCID 90012 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | HCID 13957272 | HCID 13957272 | — |
Reaktionsschritte
p-Toluenesulphonyl chloride (20.5 g) was added to a mixture of 8-chloro-1-octanol (17.7 g) and pyridine (50 ml) of 0°. After a hour the solution was added to ice and the mixture was extracted with ether. The ethereal solution was washed with dilute hydrochloric acid, dried with magnesium sulfate, and evaporated to yield the title compound as an oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04536503 |
| Quelldatensatz | uspto-grants-1985_08 |
| ORD ID | ord-b240b72b7cec4533bb47620064d06262 |
| Quellennotiz | uspto-grants-1985_08 |