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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 485299Erstellt: 24. Oktober 2026

4-Toluenesulfonyl chloride → HCID 13957272, Verbindung

https://huagongshe.com/de/reaction/485299

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-Toluenesulfonyl chlorideHCID 7397—
Edukt1-Octanol, 8-chloro-HCID 90012—
LösungsmittelPyridineHCID 1049—
ProduktHCID 13957272HCID 13957272—

Reaktionsschritte

p-Toluenesulphonyl chloride (20.5 g) was added to a mixture of 8-chloro-1-octanol (17.7 g) and pyridine (50 ml) of 0°. After a hour the solution was added to ice and the mixture was extracted with ether. The ethereal solution was washed with dilute hydrochloric acid, dried with magnesium sulfate, and evaporated to yield the title compound as an oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04536503
Quelldatensatzuspto-grants-1985_08
ORD IDord-b240b72b7cec4533bb47620064d06262
Quellennotizuspto-grants-1985_08