HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalic Acid → Zirconium phosphate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalic Acid | HCID 971 | — |
| Edukt | Phosphoric Acid | HCID 1004 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Sodium Nitrate | HCID 24268 | — |
| Edukt | Zirconyl nitrate | HCID 83761 | — |
| Produkt | Zirconium phosphate | HCID 160986 | — |
Reaktionsschritte
Oxalic acid is added to an aqueous solution of zirconium oxynitrate and sodium nitrate with stirring and phosphoric acid is further added thereto. This is adjusted to a pH of 3.5 with aqueous sodium hydroxide solution and is refluxed under heating for 78 hours and the precipitate is subjected to filtration, washing with water, drying and grinding to obtain zirconium phosphate [NaZr2 (PO4)3 ] of network structure. This zirconium phosphate is immersed in an aqueous solution containing an antimicrobial metal at a suitable concentration to obtain the phosphate of the present invention which has network structure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05296238 |
| Quelldatensatz | uspto-grants-1994_03 |
| ORD ID | ord-2019a614a96048778423ae215de8622e |
| Quellennotiz | uspto-grants-1994_03 |