[N+]([O-])([O-])=O.[Ag+:5].N.[NH:7]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[N:9]=[N:8]1>>[NH:7]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[N:9]=[N:8]1.[Ag:5]Prepared by mixing simultaneously an ammoniacal silver nitrate aqueous solution and bendotriazole (containing 0.2 mol % of aqueous ammonia per mol benzotriazole) into a 10%-aqueous solution of phenylcarbamoyl gelatin of 50° C. After completing the addition, the pH was reduced and then flocculation and desalting were carried out to obtain needle crystals (width: 0.1 to 0.2 μm, length: 0.5 to 2 μm). ##STR9##
Wird geladen…