2-Oxo-1,3-thiazolidine-4-carboxylic acid → N-(3-Nitrooxypropyl)-2-oxothiazolidine-4-carboxamide

HRID 487957

Reaktionsgleichung

Reaktionsgleichung von HRID 487957
[N+]([O-])(O)=O.[N+:5]([O:8][CH2:9][CH2:10][CH2:11][NH2:12])([O-:7])=[O:6].[O:13]=[C:14]1[NH:18][CH:17]([C:19](O)=[O:20])[CH2:16][S:15]1>>[N+:5]([O:8][CH2:9][CH2:10][CH2:11][NH:12][C:19]([CH:17]1[CH2:16][S:15][C:14](=[O:13])[NH:18]1)=[O:20])([O-:7])=[O:6]

Komponenten

3

Edukt 2

HCID 652722-Oxo-1,3-thiazolidine-4-carboxylic acidHCID 220145913-Nitroxypropylamine nitrate

Produkt 1

HCID 18961065N-(3-Nitrooxypropyl)-2-oxothiazolidine-4-carboxamideAusbeute 35,4 %

Versuchsvorschrift

A procedure similar to that described in Example 1 was repeated, but using 1.25 g of N-(3-nitrooxypropyl)-amine nitrate and 1.0 g of 2-oxothiazolidine-4-carboxylic acid, to obtain 0.60 g of the title compound as pale yellow crystals, melting at 83°-85° C.

Quellen und Nachweise

ORD-Eintrag
ord-b86c1d8036bc43feb049a8b38b5ce394
Quelldatensatz
uspto-grants-1994_03
Patentnummer
US05298516

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