4-Ethynylaniline → 2-(4-Amino-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

HRID 488475

Reaktionsgleichung

Reaktionsgleichung von HRID 488475
[CH2:1]([O:3][C:4]([C:6]1[N:7]([CH3:13])[C:8](Br)=[N:9][C:10]=1[CH3:11])=[O:5])[CH3:2].[C:14]([C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1)#[CH:15]>>[CH2:1]([O:3][C:4]([C:6]1[N:7]([CH3:13])[C:8]([C:15]#[C:14][C:16]2[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=2)=[N:9][C:10]=1[CH3:11])=[O:5])[CH3:2]

Komponenten

3

Edukt 2

HCID 37600254-EthynylanilineHCID 13897513ethyl 2-bromo-1,4-dimethyl-1H-imidazole-5-carboxylate

Produkt 1

HCID 98354742-(4-Amino-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

Versuchsvorschrift

The title compound, MS: m/e=284.4 (M+H+) was prepared in accordance with the general method of example 1b from 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester and 4-ethynylaniline.

Quellen und Nachweise

ORD-Eintrag
ord-dd23df0b12d34f938cdba6f0864d81b7
Quelldatensatz
uspto-grants-2005_12
Patentnummer
US06972299B2

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