Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Aluminum sec-butoxide | HCID 61289 | — |
| Edukt | HCID 22269484 | HCID 22269484 | — |
| Lösungsmittel | Mesitylene | HCID 7947 | — |
| Produkt | 2,9-Dihexylpentacene | HCID 17973372 | — |
Reaktionsschritte
A mixture of 1.0 grams of 3,10-dihexylpentacene-5,12-dione and 2.5 grams of aluminum tri(sec-butoxide) in 50 mL of mesitylene was heated to 155° C. for 2 days and cooled. The reaction mixture was filtered and the residue washed with concentrated HCl to give 2,9-dihexylpentacene.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US06974877B2 |
|---|
| Quelldatensatz | uspto-grants-2005_12 |
|---|
| ORD ID | ord-2c8db88bb45447ab8ec829bde259eb2e |
|---|
| Quellennotiz | uspto-grants-2005_12 |
|---|
