HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione → HCID 10408650, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione | HCID 94834 | — |
| Edukt | 4-(2-Pyrimidinyl)-1-piperazinebutanamine | HCID 12840705 | — |
| Produkt | HCID 10408650 | HCID 10408650 | 17% |
Reaktionsschritte
The title compound was prepared from 2.47 g (10.4 mmol) of 1-(4-aminobutyl)-4-(2-pyrimidinyl)piperazine and 1.89 g (10.3 mmol) of dl-camphoric anhydride, substantially according to the procedure of Example 1. This afforded 0.7 g of product, mp 94°-97° C. (17% yield).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05242911 |
| Quelldatensatz | uspto-grants-1993_09 |
| ORD ID | ord-88cb2fb8067f482b8c767b3656f1557f |
| Quellennotiz | uspto-grants-1993_09 |