HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → N'-[(2'-nitro-1,1'-biphenyl-4-yl)methyl]-N'-pentyl-N-(2,4,6-trifluorophenyl)urea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Edukt | 2,4,6-Trifluorobenzoic acid | HCID 520373 | — |
| Edukt | N-[(2'-nitro-1,1'-biphenyl-4-yl)methyl]-N-pentylamine | HCID 17860716 | — |
| Produkt | N'-[(2'-nitro-1,1'-biphenyl-4-yl)methyl]-N'-pentyl-N-(2,4,6-trifluorophenyl)urea | HCID 68850802 | 95% |
Reaktionsschritte
Using 2,4,6-trifluorobenzoic acid (0.43 g), diphenylphosphoryl azide (0.68 g), triethylamine (0.25 g) and N-[(2′-nitro-1,1′-biphenyl-4-yl)methyl]-N-pentylamine (0.40 g), N′-[(2′-nitro-1,1′-biphenyl-4-yl)methyl]-N′-pentyl-N-(2,4,6-trifluorophenyl)urea (0.60 g) was obtained by a similar procedure as in Example 4. Yield: 95%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07531576B2 |
| Quelldatensatz | uspto-grants-2009_05 |
| ORD ID | ord-ad60fc8c99314aac82cf2db2c0b61c60 |
| Quellennotiz | uspto-grants-2009_05 |