HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Fluoro-6-nitroaniline → 3-Fluorobenzene-1,2-diamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Fluoro-6-nitroaniline | HCID 87316 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 3-Fluorobenzene-1,2-diamine | HCID 2782835 | — |
Reaktionsschritte
A solution of 2-fluoro-6-nitro-phenylamine [K. L. Kirk and L. A. Cohen J. Org. Chem. 34, 384-389 (1969)] (1.05 g) in ethanol (50 ml) was hydrogenated over 10% palladium on carbon (0.5 g), filtered and evaporated to give a brown solid, used without purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07534793B2 |
| Quelldatensatz | uspto-grants-2009_05 |
| ORD ID | ord-c493ca06571448c0add5b9ae3bca65e2 |
| Quellennotiz | uspto-grants-2009_05 |