2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- → Ethyl 6-(4-fluorophenyl)-2-methylpyridine-3-carboxylate
Reaktionsgleichung
CN([CH:4]([CH3:14])[C:5]([C:7]1[CH:12]=[CH:11][C:10]([F:13])=[CH:9][CH:8]=1)=O)C.[NH2:15]/[C:16](/[CH3:23])=[CH:17]\[C:18]([O:20][CH2:21][CH3:22])=[O:19]>>[F:13][C:10]1[CH:9]=[CH:8][C:7]([C:5]2[CH:4]=[CH:14][C:17]([C:18]([O:20][CH2:21][CH3:22])=[O:19])=[C:16]([CH3:23])[N:15]=2)=[CH:12][CH:11]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared from dimethylamino-(4-fluorophenyl)propan-1-one and ethyl 3-aminocrotonate using the general procedure outlined in D18. MS (ES): MH+ 260.
Quellen und Nachweise
- ORD-Eintrag
- ord-9b3ff070b454430ca3ff0a600fe0c8a5
- Quelldatensatz
- uspto-grants-2009_05
- Patentnummer
- US07538121B2
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