Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Benzyl Chloride | HCID 7503 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 4-Cyanophenol | HCID 13019 | — |
| Lösungsmittel | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Produkt | 4-Benzyloxybenzonitrile | HCID 561371 | — |
Reaktionsschritte
A mixture containing 325 g of 4-cyanophenol, 346 mL of benzyl chloride and 758 g of potassium carbonate in 1.2 L of NMP was heated at 95° C. with stirring for 1.5 hrs. The reaction mixture was cooled to room temperature and poured into 5 L of cold water. The resulting white solid was collected, washed with water and hexanes and dried at 70° C. in vacuo giving 570.0 g of 4-benzyloxybenzonitrile.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05242924 |
|---|
| Quelldatensatz | uspto-grants-1993_09 |
|---|
| ORD ID | ord-61cb043d375d440baf6c30523544e136 |
|---|
| Quellennotiz | uspto-grants-1993_09 |
|---|
