HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-3,3-dimethylbutanamide → (2R)-2-Amino-3,3-dimethylbutanamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-3,3-dimethylbutanamide | HCID 3496444 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | (2R)-2-Amino-3,3-dimethylbutanamide | HCID 10197708 | — |
Reaktionsschritte
In accordance with the process described in JP Patent Application Laying Open (Kokai) No. 62-55097, Enterobacter cloacae N-7901 (FERM BP-873) was cultured. 1 L of culture solution was centrifuged, and the wet cells were then suspended in distilled water to prepare a 800 g cell suspension. 200 g of D,L-tert-leucine amide was dissolved in this suspension, and the solution was then allowed to react at 40° C. for 52 hours. After the reaction, cells were removed by centrifugation and 970 g of an aqueous solution containing 10% by mass each of L-tert-leucine and D-tert-leucine amide was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06949658B2 |
| Quelldatensatz | uspto-grants-2005_09 |
| ORD ID | ord-a6931ace804f4de0aea194ee160ea841 |
| Quellennotiz | uspto-grants-2005_09 |