HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HCID 67530783, Verbindung → HCID 67529444, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | HCID 67530783 | HCID 67530783 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Katalysator | Platinum oxide monohydrate | HCID 86587499 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 67529444 | HCID 67529444 | — |
Reaktionsschritte
This compound was prepared in a manner analogous to that of Step E of Example 1, by the hydrogenation of 0.5 gram (0.0022 mole) of 3-(imidazol-5-yl)-5-methoxy-6-methylindene (viii) in the presence of 0.1 gram (catalyst) of 10% palladium on carbon and 0.1 gram (catalyst) of platinum oxide hydrate in 40 mL of ethanol. The yield of subject compound was 0.42 gram, mp 68-70° C. The NMR spectrum was consistent with the proposed structure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07767667B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-ddef700dccce4e6487c6d9dacbbe1683 |
| Quellennotiz | uspto-grants-2010_08 |