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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 499022Erstellt: 25. Oktober 2026

HCID 67530783, Verbindung → HCID 67529444, Verbindung

https://huagongshe.com/reaction/499022

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHCID 67530783HCID 67530783—
KatalysatorPalladiumHCID 23938—
KatalysatorPlatinum oxide monohydrateHCID 86587499—
LösungsmittelEthanolHCID 702—
ProduktHCID 67529444HCID 67529444—

Reaktionsschritte

This compound was prepared in a manner analogous to that of Step E of Example 1, by the hydrogenation of 0.5 gram (0.0022 mole) of 3-(imidazol-5-yl)-5-methoxy-6-methylindene (viii) in the presence of 0.1 gram (catalyst) of 10% palladium on carbon and 0.1 gram (catalyst) of platinum oxide hydrate in 40 mL of ethanol. The yield of subject compound was 0.42 gram, mp 68-70° C. The NMR spectrum was consistent with the proposed structure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07767667B2
Quelldatensatzuspto-grants-2010_08
ORD IDord-ddef700dccce4e6487c6d9dacbbe1683
Quellennotizuspto-grants-2010_08