Hydrochloric Acid → 2-Aminoquinoline-6-carboxylic Acid Hydrochloride
Reaktionsgleichung
[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:12]([O:14]CC)=[O:13])[CH:8]=2)[N:3]=1.[ClH:17]>>[ClH:17].[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:12]([OH:14])=[O:13])[CH:8]=2)[N:3]=1Komponenten
3
Versuchsvorschrift
330 mg of ethyl 2-aminoquinoline-6-carboxylate was stirred in 30 ml of 6 M hydrochloric acid at 80° C. overnight. The solvent was evaporated, and the residue was washed with ethyl acetate to obtain the title compound.
Aufarbeitung
- customThe solvent was evaporated
- washthe residue was washed with ethyl acetate
Quellen und Nachweise
- ORD-Eintrag
- ord-433f363192db47b18bcac0f46394763f
- Quelldatensatz
- uspto-grants-2004_03
- Patentnummer
- US06710056B2
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